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- Procedure: Step 1: Pipet 25 mL of prepared sample solution, which has been prepared into a 250 mL Erlenmeyer flask. Step 2: Add 3-5 drops of phenolphthalein indicator solution to the sample solution in the 250 mL Erlenmeyer flask. Step 3: Rinse the buret with three 10 mL portions of standardized 0.1 M HC1 acid solution, before fill this acid solution into the buret and record the initial volume of this acid solution in the burette. Step 4: Titrate the sample solution with the standardized 0.1 M HC1 to the endpoint and record the final volume of this acid in the burette. (Note: phenolphthalein endpoint is from pink color to colorless) Step 5: Repeat the titration for two more times. Step 6: Repeat the same procedure from step 1 to step 5 by using methyl orange as an indicator rather than phenolphathelein. (Note: methyl orange endpoint is from orange to red color). Calculate the alkalinity of the sample for both the indicators and potentiometric method using the following equation: [Alk]…1. Develop a detailed separation scheme for the separation and determination of the percent composition of your sample which will be a mixture of NaCl, NH.CL, and sand. You are expected to use the properties of the components listed below and some of the techniques listed in the table in the pre-lab queries (and used in Separations I). Keep in mind that any chemistry student should be able to pick up your scheme, understand it, and use it to complete the separation and calculation of % composition. Place the scheme on a separate sheet of paper. Component Solubility (@25°C) Melting Point Hardness sodium chloride, NaCl 35 g/100 mL water 801°C soft ammonium chloride, NH&Cl 37 g/100 mL water sublimes 350°C soft sand, SIQ2 insoluble 1600°C hard Example of compounds in a container. Naci NH.CI sio2 Exploring the Chemical World, PGCC, 2003 4 RESULTS Show all calculations with units in this space.Current Attempt in Progress From the curves shown in Animated Figure and using the following Equation, determine the rate of recrystallization for pure copper at the several temperatures. Make a plot of In(rate) versus the reciprocal of temperature (in K-1). (a) Determine the activation energy for this recrystallization process. (See Section FACTORS THAT INFLUENCE DIFFUSION.) (b) By extrapolation, estimate the length of time required for 50% recrystallization at room temperature, 20°C (293 K). (a) i kJ/mol (b) i days
- The following volumes of 0.000300 M SCN are diluted to 15.00 mL. Determine the concentration of SCN in each sample after dilution. These values will be used during the experiment. To enter exponential values, use the format 1.0e-5. Sample 0.000300 M SCN (mL) [SCN'] (M) 1 1.50 3.50 7.00 4 10.00 3.The following volumes of 0.000300 M SCN- are diluted to 15.00 mL. Determine the concentration of SCN- in each sample after dilution. These values will be used during the experiment. Sample 0.000300 M SCN- (mL) [SCN-] (M) 1 1.50 2 3.50 3 7.00 4 10.00Complete the table and provide the percent (%) recovery for each extraction.
- B. Determining the Composition of a Mixture of Sodium Chloride and Sodium Nitrate Partner I Prepare a solution of sodium chloride + sodium nitrate and indicator. Obtain a dropper bottle of potassium chromate (indicator) solution. To a clean and dry 125 mL Erlenmeyer flask, add about 40 mL of water and 8 drops of indicator solution. Weigh out approximately 0.05 grams of sodium chloride + sodium nitrate solid and record its exact mass. Dissolve the solid in the solution from step 1, stirring with a stirring rod to ensure complete dissolution. Determine and record the total mass of the Erlenmeyer flask and solution, noting the balance that you use to weigh. Rather than measuring the volume of silver nitrate solution added as in Part A, we will measure the mass of titrant added and make use of the weight-percentage concentration of silver nitrate in calculations. Prepare the silver nitrate solution. Obtain about 15 mL of 1.70% w/w silver nitrate solution in a 50 mL beaker. Designate a…You want to determine the concentration of NaCl in a water. In preliminary analysis, it appears to be saline water with a NaCl content of approximately 4%. Should you dilute the sample if your titrant has a concentration of 0.1 M and you want to spend 25 mL of sample? Solution: You must dilute approximately ten times, taking 10 mL of sample and making up to 100 mL. In this way, 17.20 mL of titrant will be spent.Complete the table by entering the molarity of B2- for each standard solution. Show an illustrative calculation for tube ‘A’. Use the dilution formula and express each result to one more digit than allowed by applying the rules of significant figures. Standard Volume of stock B2- solution taken, mL Molarity of dilute B2 Construct a graph of Absorbance vs. molarity of B2- in Excel using the data in the preceding table. Make certain to title the graph and include axes labels with proper units. Absorbance is dimensionless (has no unit). Add a linear trendline to the graph but do not set the y-intercept to zero Solid M2B is added to 25 mL of water, the resulting mixture is continually stirred for 1 hour. At this point, it is assumed that equilibrium (eqn 3) has been established. The mixture is transferred to a test tube, and the test tube is centrifuged to assure that any residual solid M2B is fully settled out. A portion of the supernatant in the test tube is carefully…
- Weigh out accurately 9.99 g of copper(II) sulfate pentahydrate (CuSO4·5H2O) by taring using a clean and dry empty 250-ml beaker. 2. Add tap water to the beaker to reach the 50-mL mark on the side of the beaker. 3. Dissolve all the crystals of CuSO4·5H2O in the water using a clean glass rod for stirring. 4. Then using a glass funnel transfer all the blue solution to a 100-mL volumetric flask. Rinse the beaker with about 10 mL of water and transfer the solution to the volumetric flask. Repeat the rinsing of the beaker with another 10 mL of water and transfer the solution to the volumetric flask. This is called quantitative transfer of the solution. 5. Then add enough water to reach the calibration mark of the volumetric flask. (You will need to use a dropper to add the last few drops of water to ensure the meniscus is on the calibration mark). Close the volumetric flask with a stopper and mix the solution well (so that it is homogeneous). 6. You have now prepared a standard solution (or…You obtain an Unknown Sample from the Stockroom. You begin testing the solution through the steps outlined in the flowchart of the experiment’s PDF file. You first add HCl and centrifuge your mixture. You observe the formation of a white precipitate in the bottom of the test tube. After pouring off the supernatant liquid, you add hot water to the white precipitate. Upon addition of the hot water, you have some white precipitate still at the bottom of the test tube, and the supernatant liquid is poured off. To this liquid, potassium chromate (K2CrO4) is added. Upon this addition of potassium chromate, you observe no formation of precipitate. Which of the following is a valid conclusion to draw at this point? (Choose one.) Select one: 1. Hg22+ is definitely present. 2. Pb2+ is NOT present. 3. Ag+ is definitely present. 4. Pb2+ is definitely present.You want to make a solution of the primary standard sodium oxalate. It has a molecular mass of 133.999 g/mol (no error). Your analytical balance has an error of 0.2 mg. You add some weighing paper to the balance and it reads a mass of 0.23626 g. You then add sodium oxalate onto the weighing paper until the mass registers as 2.8539 g. You carefully transfer this to a 250.0 ml volumetric flask with an error of 0.1 ml and dissolve the sodium oxalate in a sufficient volume of water. What is the concentration of the oxalic acid (in M) and what is the absolute error (also in M).