EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
6th Edition
ISBN: 9781305687875
Author: Gilbert
Publisher: CENGAGE LEARNING - CONSIGNMENT
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Question
Chapter 3.3, Problem 1E
a)
Interpretation Introduction
Interpretation:Errors in procedure that cause observed melting point of pure compound to be lower than correct melting point should be determined.
Concept introduction:Melting point is temperature that involves conversion of substance from solid to liquid state. Both liquid and solid phases are present in equilibrium with each other at this temperature.
b)
Interpretation Introduction
Interpretation:Errors in procedure that cause observed melting point of pure compound to be higher than correct melting point should be determined.
Concept introduction:Melting point is temperature that involves conversion of substance from solid to liquid state. Both liquid and solid phases are present in equilibrium with each other at this temperature.
c)
Interpretation Introduction
Interpretation:Errors in procedure that cause observed melting point of pure compound to be broad in range than correct melting point should be determined.
Concept introduction:Melting point is temperature that involves conversion of substance from solid to liquid state. Both liquid and solid phases are present in equilibrium with each other at this temperature.
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1. Total Milk solids = 12.2% H20 = 87.8%
Milk standardized solids = 8.8% Butterfat
solids = 3.4% solids
a. Find out what the freezing point is for the
milk.
b. If you cool the milk slowly to -5 C°, describe
what phases form in your milk bottle.
c. Calculate the relative fraction of the phases
in (b).
Chemistry
5. You melt the substance and de-coloration occurs. Unfortunately, you weren’t paying attention and miss the melting point. Should you start over or re-melt it? Or both are options ‘okay’?
6. When measuring the melting point of a substance, it suddenly disappears. What has happened? Can you still measure the melting point? If so, how?
7. We should not re-use a sample in a capillary tube for melting point measurement. Why not?
8. It takes significant amount of time for the melting point apparatus to cool down before next measurement if your new sample has a lower melting point than your previous one. What can you do to reduce this time in between measurements when many samples of different melting points are used?
Which of the melting point capillaries in the picture below is filled to the proper
level for taking a melting point on a MelTemp melting point apparatus?
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OC
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Chapter 3 Solutions
EBK EXPERIMENTAL ORGANIC CHEMISTRY: A M
Ch. 3.2 - Prob. 1ECh. 3.2 - Prob. 2ECh. 3.2 - Prob. 3ECh. 3.2 - Prob. 4ECh. 3.2 - Prob. 5ECh. 3.2 - Prob. 6ECh. 3.2 - Prob. 7ECh. 3.2 - Prob. 8ECh. 3.2 - Prob. 9ECh. 3.2 - Prob. 10E
Ch. 3.2 - Prob. 11ECh. 3.2 - Prob. 12ECh. 3.2 - Prob. 13ECh. 3.2 - Prob. 14ECh. 3.2 - Prob. 15ECh. 3.2 - Prob. 16ECh. 3.2 - Prob. 17ECh. 3.2 - Prob. 18ECh. 3.2 - Prob. 19ECh. 3.2 - Prob. 20ECh. 3.2 - Prob. 21ECh. 3.2 - Prob. 22ECh. 3.2 - Prob. 23ECh. 3.2 - Prob. 24ECh. 3.2 - Prob. 25ECh. 3.2 - Prob. 26ECh. 3.2 - Prob. 27ECh. 3.2 - Prob. 28ECh. 3.2 - Prob. 29ECh. 3.2 - Prob. 30ECh. 3.2 - Prob. 31ECh. 3.2 - Prob. 32ECh. 3.2 - Prob. 34ECh. 3.3 - Prob. 1ECh. 3.3 - Prob. 2ECh. 3.3 - Prob. 3ECh. 3.3 - Prob. 4ECh. 3.3 - Prob. 5ECh. 3.3 - Prob. 6ECh. 3.3 - Prob. 7ECh. 3.3 - Prob. 8ECh. 3.3 - Prob. 10ECh. 3.3 - Prob. 11ECh. 3.3 - Prob. 12ECh. 3.3 - Prob. 13ECh. 3.3 - Prob. 14ECh. 3.3 - Prob. 15ECh. 3.3 - Prob. 16ECh. 3.3 - Prob. 17ECh. 3.3 - Prob. 18ECh. 3.3 - Prob. 19ECh. 3.3 - Prob. 21ECh. 3.3 - Prob. 22ECh. 3.3 - Prob. 23ECh. 3.3 - Prob. 24ECh. 3.3 - Prob. 25ECh. 3.3 - Prob. 26E
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