OUROUTUISHIRT amide (1°) 4000 10 9.0 3500 NH 8.0 CH (sp³) 3000 1 1 7.0 Molecule 10 2500 6.0 2000 wavenumber (cm-¹) 5.0 4.0 1500 3.0 2 2.0 1000 2 (sextet) 1.0 3 500 0.0
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- Intensity (a.u.) 4000 3352 cm¹ 3500 3000 UNKNOWN B 1710 cm¹ 2000 1668 cm¹ 2500 Wavenumber (cm¹¹) 1500 1101 cm 1000 5001. C5H1002 10 HPM-00-297 100 TRANSMITERE 9 4000 8 T 3000 T 7 T 6 2000 5 ppm MOVENEDI T 4 3 T 1500 : T 3 1 T 2 : T 1000 6 T 1 T 0 500 200 DEPT-90 180 160 CDS-00-156 DEPT-135 140 120 100 ppm T 80 60 T 40 20 لندChemistry Question
- 1. Each of the following IR spectra is associated with one of the aromatic compounds below. Identify the compound associated with each spectrum. N. H HO a-tetralone B-tetralone 2-indanone N-methylbenzamide m-cresol Spectrum A MICRONS NICOLET 20SX FT-IR 2.8 2.9 2.5 100 2.6 2.7 3.5 4 4.5 5.5 7 10 11 12 13 14 15 16 17 18 19 21 22 0.0 90 .05 80 0.1 70 % 0.2 60 50 0.3 40 0.4 0.5 30 -0.6 20 0.7 0.8 0.9 1.0 2.0 4000 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 600 450 WAVENUMBERS Spectrum B MICRONS NICOLET 20SX FT-IR 2.5 100 2.6 2.7 2.8 2.9 3 3.5 4 4.5 5.5 7 8 10 11 12 13 14 15 16 17 18 19 21 22 + 0.0 90 .05 80 0.1 70 % 0.2 60 50 -0.3 B 40 0.4 E 0.5 30 0.6 20 0.7 0.8 0.9 10 1.0 2.0 4000 3800 3600 3400 3200 3000 2800 2600 2400 2200 2000 1800 1600 1400 1200 1000 800 600 450 WAVENUMBERS This work by Dr. James S. Nowick, Professor of Chemistry, University of California, Irvine, is licensed under a Creative Commons Attribution 4.0 International License. Spectra…Lrdocaine USP (ATR) 95- 90 85 80 75 70 65 60 55 50 45 Lidocaine 40 4000 3500 3000 2500 2000 1500 1000 Wavenumbers (cm-1) %Transmittance IZ 3243.36 3021.30 2968.47 2921.13 2799.39 1661.66 1593.98 1491.43, 1449.061 422.12,384.681371.62 1291.03264.55 1206.99 1165.931119.56 1091.78072.77. 1034.33 970.79986.39 917.91, 885.23 763.76 703.94 615.01599.90Following are infrared spectra of 2-methyl-1-butanol and tert-butyl methyl ether. Assign each compound its correct spectrum. Micrometers 2.5 100 3. 4. 9. 13 8 10 11 12 14 15 20 90 80 70 50 40 30 20 10 4000 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 600 400 Wavenumber (cm-1) Transmittance (%)
- % transmittance alkane 4000 2.0 1.8 3500 1.6 CH (sp³) 3000 1 (nonet) .... 1.4 Molecule 2 2500 2000 wavenumber (cm-¹) 1.2 6 (doublet) 2 (quintet) 1.0 8 (ppm) 3 (triplet) 0.8 1500 0.6 0.4 1000 0.2 500 0.0You will check the outcome of reaction via infra-red spectroscopy: what are the diagnostic functional group peaks for the following compounds? You should also indicate the stretching motions responsible for absorbance. Dilantin benzil (unreacted starting material) Urea (unreacted starting material)% TRANSMITTANCE 100- 88 28 4800 35.88 3350.18 ( 5H 3028.63 2983.84 3888 MITT 8.0 7.5 7.0 PPM Proton NMR 140 Carbon 13 NMA 120 2874.30 2588 100 HAVENUMBERS 2H 3.5 2008 3.0 80 1H 1603.05 1383.14P 145258 1588 2.5 1033.98 1012.76 1888 2.0 86-10931094 781. 1H 3H MF C₂H120 MW 136 !!! 60 40 20 PPM %C 79.4 1.5 PPM 1.0 %H 8.9 0
- Transmittance (%) Transmittance (%) 100 50 4000 100 4000 3000 2000 1500 Wavenumber(cm¹) 1500 Wavenumber(cm¹) 1000 1000 5006. C8H100 11 TRANSMITTANCE LOD HSP-04-492 0+ 10 4000 9 3000 8 5 7 6 : 5 ppm 2000 4 HAVENUMBERI-l 2: 2 1 3 1500 2 سهر 1 1000 0 500 200 T 180 CDS-06-431 DEPT-90 T 160 DEPT-135 140 120 100 لك -2 peaks u ppm 80 60 40 20 03. 11 100 TRANSMETTANCE D C8H9CIO 4000 10 HSP-01-151 9 3000 8 2:2 7 2000 6 : 5 ppm 2 NAVENUMBERal 4 3 1500 : Vala 2 1000 3 1 0 500 200 180 COS-04-715 DEPT-90 DEPT-135 160 140 120 بلد لد 100 ppm 80 60 40 20 0