Example: For the synthesis of adipic acid from cyclohexanone, 1.0 mL of nitric acid and 0.154 g of cyclohexanone were used initially. Following the reaction, 0.325 g of crude product was isolated as light yellow clumps, with a mp range of 145-150 °C. This crude product was purified by recrystallization to yield 0.173 g of pure product (off-white crystals), with a mp range of 151-153 °C. A typical yield of adipic acid is 0.190 g. Use the space provided to write out the Results and Discussion sections that would appear in a lab report for this experiment. 8 1.0nL 0.1540 0.3259 HNO, 145-150°C COOH COOH C 0.1739 151-15342

Example: For the synthesis of adipic acid from cyclohexanone, 1.0 mL of nitric acid and 0.154 g of cyclohexanone were used initially. Following the reaction, 0.325 g of crude product was isolated as light yellow clumps, with a mp range of 145-150 °C. This crude product was purified by recrystallization to yield 0.173 g of pure product (off-white crystals), with a mp range of 151-153 °C. A typical yield of adipic acid is 0.190 g. Use the space provided to write out the Results and Discussion sections that would appear in a lab report for this experiment. 8 1.0nL 0.1540 0.3259 HNO, 145-150°C COOH COOH C 0.1739 151-15342

Macroscale and Microscale Organic Experiments

7th Edition

ISBN:9781305577190

Author:Kenneth L. Williamson, Katherine M. Masters

Publisher:Kenneth L. Williamson, Katherine M. Masters

Chapter7: Extraction

Section: Chapter Questions

Problem 1Q

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