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- 2. Provide synthetic route for the following transformation mia CIInstructions. Briefly describe the following given reactions. 2. The conversion of benzaldehyde into benzophenone. HNO, SOCL, (Oxidation) Benzaldehyde (Friedel-Craft acylation) Anhyd. AICI, Benzophenone AN SWERS: Desk1) Show how m-toluidine (shown on the right) can be converterd to the following compounds using any neccesary reagents. (You can use a previously synthesized compound to carry on). a) H₂C- b) d) c) H₂C m-toluonitrile m-iodotoluene H₂C. CN m-cresol CHÍNH, OH H₂C.
- Two possibilities for a Wittig synthesis of the compound below involve using: 1)cyclohexanone and ethyl bromide or 2) bromocyclohexane and ethanal. Is either routebetter, and if so, why is one superior? Be specific and explain where the difficulty lies forthe inferior routeIdentify the reagents necessary for all three methods. ? OH ajay O CH3CH₂ONa ? ? 1) NaOH; 2) CH3CH₂OH CH3CH₂OH, H₂SO4 1) NaOH; 2) CH3CH₂Br OCH3CH₂Br, H₂SO4 □1) SOCI₂; 2) CH3CH₂OH, pyridine OEtOthesis. teps neceossary to synthesize this compound by yl halide; after that you can add any organic or Dound. →1-hexanol )Consider the following compounds: B = HOCH2CH2CH2CH3 CH3 HC C = CH3CH2CH2OCH2CH2CH3 D = a) Which one(s) could be reduced with NaBH4? b) Which one(s) would give a positive Tollens silver mirror test? c) Which one(s) could be oxidized with CrO3? d) Which one(s) would react with 1 or 2 equivalents CH3M9B to make a npound butyl ethyl ether larger alcohol?
- . Propose a plausible arrow pushing mechanism for the following transformation8. Outline a reasonable synthesis for the following molecule given the indicated starting material. You may use any reagent/s necessary. You must show all intermediate products. a. OH O M741-Group09. OrmordTo preview image click here ↓ Perform the retrosynthetic analysis for the indicated bond and choose the correct synthetic equivalents. A. B. O A B D : OMe + :0: + NaOMe + NaOMe C. D. MeO +ÖMe + NaOH NaOH
- (b) do Using the reagents below, list in order (by letter, no period) those necessary to prepare compound B from Note: Not all spaces provided may be needed. Type "na" in any space where you have no reagent. a. Ethyne b. NaC=CH₂ c. NaCCH d. NBS, light e. HCN f. NaCN g. NaOEt, EtOH Step #1 Step #2 ee Step #3 naWhich reagents can be used to achieve synthesis of the indicated target molecule? Conc. KMNO4/ H* / acetone 1) O3/ Zn/H* 2) PCC/CH2Cl2 O 1) Conc. KMNO4 /H* 2) LIAIH4/THF 4) H3O* 1) Conc. KMNO4, 2) HBr, 3) Mg/ether, 4) CO2 O3/ Zn/H*9. Provided is target molecule E and the corresponding synthetic equivalents from a proposed retrosynthetic analysis. a. Propose a reasonable forward synthesis that produces E and uses each synthetic equivalent. ezza E H SE-1 OH SE-2 SE-3