d) The following data was obtained from the determination of lead, Pb in a wastewater sample. Four measurements were made. The set of data obtained was as follow: Measurement 1 2 3 4 3 14.1 15.2 14.9 15.4 Pb concentration (ppm) i) Using Q-test, justify whether the outlier should be rejected or accepted at 90% confidence level. ii) Calculate the mean and standard deviation of the data set after the Q-test has been done. iii) Determine the 90% confidence limit for the true concentration of Pb in the sample.

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter7: Statistical Data Treatment And Evaluation
Section: Chapter Questions
Problem 7.13QAP
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Basic Analytical Chemistry - Evaluation of experimental data
d) The following data was obtained from the determination of lead, Pb in a wastewater
sample. Four measurements were made. The set of data obtained was as follow:
Measurement
1
2
3
4
3
14.1
15.2
14.9
15.4
Pb concentration
(ppm)
i) Using Q-test, justify whether the outlier should be rejected or accepted at 90%
confidence level.
ii) Calculate the mean and standard deviation of the data set after the Q-test has been
done.
iii) Determine the 90% confidence limit for the true concentration of Pb in the sample.
Transcribed Image Text:d) The following data was obtained from the determination of lead, Pb in a wastewater sample. Four measurements were made. The set of data obtained was as follow: Measurement 1 2 3 4 3 14.1 15.2 14.9 15.4 Pb concentration (ppm) i) Using Q-test, justify whether the outlier should be rejected or accepted at 90% confidence level. ii) Calculate the mean and standard deviation of the data set after the Q-test has been done. iii) Determine the 90% confidence limit for the true concentration of Pb in the sample.
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