1,8-Cineole is a predominant terpene found in cranberries. The concentration of 1,8-cineole in cranberries was determined using gas chromatography. A 5.00 g sample of freeze-dried cranberry powder was added to 10.0 mL waterto form a cranberry extract. The extract was filtered. A 1.00 mL aliquot was added to a 25 ml volumetric along with a known amount of internal standard (d-14 cymene) and diluted to volume with water. Standards were spiked with afixed amount of d-14 cymene as internal standard. The following data was obtained:1,8-Cineole (ug/mL); 1,8-Cineole (peak area); d-14 cymene (peak area)10.0; 1260; 188015.0; 1865; 185020.0; 2520; 185550.0; 6280; 1865Sample; 1976; 1840What is the concentration of 1,8-cineole in ug per gram of cranberry?O 398 ug/gO 159 ug/gO 674 ug/gO 796 ug/gO 15.9 ug/g

Concentration of 1,8 cineole is calculated as given below.

Answered: 1,8-Cineole is a predominant terpene…

Chemistry

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Chapter1: Chemical Foundations

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6.0 mL of cyclohexanol, 8 mL of 85% phosphoric acid, and 10 drops of sulfuric acid are added to a 50-mL round-bottom flask with boiling chips, and the mixture is distilled into an ice-cooled receiver. The distillate is in the form of a colorless bi-phasic mixture. The cyclohexene upper layer is removed from the water layer, and dried over anhydrous calcium chloride. Isolated is cyclohexene as a clear and colorless foul-smelling liquid. Weighing data is given below. Gross mass: 51.24 g Tare mass: 48.04 g Product mass: 3.2g Question: Calculate the theoretical mass of the cyclohexene product, bearing in mind that the cyclohexanol starting material was measured by volume, not by mass (so you must use the density of cyclohexanol to convert milliliters to grams, before calculating the number of moles). Calculate the percent yield of cyclohexene obtained.
Upon screening with TLC (made of silica gel) chromatography using hexane/chloroform (3:1) as eluting solution, 3 spots were detected corresponding to a (A) polyphenol, a (B) tannin and an (C) alkaloid. Write the letters of your answers on the spots in the chromatogram shown at the right.
2. Consider the following example GC Chromatogram from a publication about aggression among Mediterranean Acrobat Ants (C. scutellaris). This particular sample was generated by rinsing hydrocarbons from ant exoskeletons. From the chromatogram, what is the minimum number of unique compunds present in the sample? What data led you to that conclusion? (Don't overthink it) 2 8000000 7000000 6000000 5000000 4000000 3000000 2000000 1000000 Counts (Abundance) 5 19 6 7 0 23.00 24.00 10 | 11 13 17 20 14 15 16 12 teel | 22 19 21 ли 25.00 26.00 27.00 Time "Example of a Gas chromatography-Mass spectrography (GS-MS) chromatogram of hydrocarbon molecules in C. scutellaris" by Filippo Frizzi, et.al, in PLoS One is licensed under CC BY 4.0
To determine the soil distribution coefficient (Kd), 10 g of dry soil is spiked with 100 mg of ring-labeled 14C-atrazine, 10 mL of deionized water is added, and the system is shaken for 24 hours. The aqueous and solid phases are separated, and the solid phase is extracted with 50 mL of methylene chloride while the aqueous phase is extracted with three successive 5 mL portions of methylene chloride. The atrazine concentration in the 50 mL of soil extract is 10 mg/L, and the concentration in the combined 15 mL from the aqueous extractions is 0.4 mg/L. Based on this information, calculate Kd.
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If 15 mL of dichloromethane was used at one time for extraction, will the amount of the substance extracted be the same as, lesser than, or greater than that if three-5 mL fractions were used? Justify your answer by showing calculations. Assume the mass of the sample to be used is 1.0 g, volume of water is 100 mL and the KD is 5
Twenty grams of tea leaves was extracted with 250.0 mL water. The aqueous extract was then subjected to liquid-liquid extraction using a total volume of 50 mL chloroform organic solvent.
An enzymatic method for determining alcohol in the wine is evaluated by comparison with a gas-chromatography (GC) method. The same sample is analyzed several times by both methods with the following results (% ethanol). The values of alcohol for both enzymatic and GC methods are shown in Table 1. Using a suitable test, determine whether the enzymatic method gives the same value as the GC method at 95% confidence level.
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