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Discuss low percentage yield in the preparation of p-Nitroaniline.
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- You started with 84g of aniline and 28 ml of acetic anhydride. Give % yield of acetanilide. 12:04 PM 10/23/2021 白Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample. The stated should be 104.5, how??Oral rehydration salts are stated to contain the following components: Sodium Chloride 3.5g Potassium Chloride 1.5g Sodium Citrate 2.9g Anhydrous Glucose 20.0g 8.342 g of oral rehydration salts are dissolved in 500 ml of water. 5 ml of the solution is diluted to 100 ml and then 5 ml is taken from the diluted sample and is diluted to 100 ml. The sodium content of the sample is then determined by flame photometry. The sodium salts used to prepare the mixture were: Trisodium citrate hydrate (C6H5Na3O7, 2H2O) MW 294.1 and sodium chloride (NaCl) NW 58.5. Atomic weight of Na = 23. The content of Na in the diluted sample was determined to be 0.3210 mg/100 ml. Determine the % of stated content of Na in the sample.
- When a Vitamin C (ascorbic acid; MM = 176.12 g mol-1) tablet is crushed, dissolved and titrated with 0.0340 M KIO3(aq) to a purple/blue endpoint (given by a starch indicator), the volume of KIO3 used is 29.80 mL. If 60 mg of ascorbic acid is the recommended dietary allowance (i.e., 100% of the RDA), then what is the % RDA for the Vitamin C in the tablet? KIO3(aq) + 5 KI + 6 H+ → 3 I2(aq) + 3 H2O I2 (aq) + ascorbic acid → 2 I- + dehydroascorbic acidThe mixture contains benzoic acid, 2-napthol, and naphthalene. Dissolve the mixture in the polar solvent ether. When you react the mixture with 10% NaHCO3(sodium bicarbonatea weak base in aqueous solution) reacts with benzoic acid and forms sodium benzoate an ionic compound (similar to NaCl) that dissolves in aqueous solution (heavier than ether in density) and goes to the bottom of the centrifuge tube or to the bottom of the separatory funnel forming two layers. Then remove the bottom aqueous layer and collect in a beaker labeled as bicarbonate extract. Acidify the bicarbonate extract in the beaker to give benzoic acid. The top ethereal layer contains in the centrifuge tube or separatory funnel 2-napthol and naphthalene. To this top layer add 10% NaOH (sodium hydroxideis a strong base in aqueous solution reacts with only 2-napthol, a weak acid forming 2-napthoxide an ionic compound soluble in aqueous solution (similar to NaCl) that goes to the bottom of the centrifuge tube or to…How much of the suspending agent is needed to prepare a 60-mL preparation of Aluminum hydroxide gel based on this formulation? Ammonium alum 800 g Sodium carbonate 1000g Peppermint Oil 0.01% (0.01 g/100mL) Sodium benzoate 0.1% (0.1 g/100mL) Purified water, qs ad. 2000 mL a. 0.06 g b. 30 g c. 24 g d. 0.006 g
- Which ONE of the following is the correct amount of hydrocortisone contained in 50g of 0.5% (w/w) cream? 5g 2g 1g 0.25g 0.125g А. В. С. D. Е.The following compounds are available as 0.10 M aqueous solutions: pyridine triethylamine m-nitroaniline NaOH phenol HCIO HCIO4 (рКь = 8.82) (pKb = 3.25) (pKb = 11.53) (K₂ = 1.1 × 10-10) (K₂ = 2.9 × 10-8) Which two solutions could be combined to prepare a pH 6.7 buffer? HCIO and NaOH phenol and NaOH m-nitroaniline and HCIO4 pyridine and HCIO4• How many grans and how many mL of 40.0 wt-% urea solution (density 1.111 g/mL) are required to react with 4.00 mol of Fe3+ in the following reactions? • (H2N)2CO + 3 H2O → CO2 + 2 NH4+ + 2 OH- Fe3+ +3 OH- + (x-1)H2O - FEOOH x x H2O(s)
- In what proportion may the Manufacturing pharmacist mix 20%, 15%, 5% and 3% ZnO to produce 10% ZnO ointment?Concentration of Reagents (NH4)2S2O8 KI Na2S2O3 0.25 M 0.22 M 0.19 M Volumes of Solutions S₂082 (mL) Starch soln (mL) KNO3 (mL) EDTA soln (mL) KI (mL) S₂O32- (mL) x 5 9.7 0.9 26.4 0.5 9.9 1.1 Using the above data determine the concentration of I at the moment the reaction begins. HINT: This is a mixing problem. Determine the total number of moles of I and divide this amount by the total volume (in L). Be careful... If you go back and try this exercise again the values will change. Read the question carefully! Answer:During your first day on the job as a research assistant, you are preparing 50 mL of hybridization solution with the following components and working concentrations: 50% formamide 5X sodium salt citrate 0.5% sodium dodecyl sulfate You start from the following concentrated stock solutions: 100% formamide 20X sodium salt citrate 20% sodium dodecyl sulfate How much of each concentrated stock solution and water will you add?