Q1:What effect would each of the following have on the observed melting point and melting point range of a sample: .Use of a thick-walled melting point tube (a) .Rapid heating (b) Use of so much sample that the filled (c) portion of the capillary tube extends considerably beyond the thermometer .bulb .Presence of solvent within the crystal (d) Presence of piece of glass in the sample (e) Q2: Why melting point are routinely used?

Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter3: Melting Points And Boiling Points
Section: Chapter Questions
Problem 12Q: An unknown compound is suspected to be acetanilide (mp113.5-114C). What would happen to the melting...
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Q1:What effect would each of the following
have on the observed melting point and
melting point range of a sample:
.Use of a thick-walled melting point tube (a)
.Rapid heating (b)
Use of so much sample that the filled (c)
portion of the capillary tube extends
considerably beyond the thermometer
.bulb
.Presence of solvent within the crystal (d)
Presence of piece of glass in the sample (e)
Q2: Why melting point are routinely used ?
Q3: Why and how the Thermometer
calibration ?
Q4: Draw the temperature composition
diagram for the following data:
melting point
compound
150
Pure A
187
Pure B
112
A:50% B 50%
170
A:80% B 20%
146
A: 20% B 80%
Transcribed Image Text:Q1:What effect would each of the following have on the observed melting point and melting point range of a sample: .Use of a thick-walled melting point tube (a) .Rapid heating (b) Use of so much sample that the filled (c) portion of the capillary tube extends considerably beyond the thermometer .bulb .Presence of solvent within the crystal (d) Presence of piece of glass in the sample (e) Q2: Why melting point are routinely used ? Q3: Why and how the Thermometer calibration ? Q4: Draw the temperature composition diagram for the following data: melting point compound 150 Pure A 187 Pure B 112 A:50% B 50% 170 A:80% B 20% 146 A: 20% B 80%
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