Procedure: 0.0402 g of water was titrated with Fisher's reagent according to the pharmacopoeial procedure. 10.05 ml was used for titration, 0.5 ml for the control experiment (blank run). Calculate the titrimetric conversion factor (T) for this solution using above- mentioned formula.
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- 10) 1.0 gram of CaCO3 was dissolved in HCl and the solution was made up to 1000 ml with distilled water. 50 ml of the solution required 45 ml of EDTA solution for titration, 50 ml of hard water sample required 28 ml of EDTA and after boiling and filtering required 15 ml of EDTA solution. Calculate Temporary Hardness. A. 288.6 ppmB. 166.6 ppmC. 88.6ppm 11) Calculate the Permanent Hardness for No. 10 A. 111 ppmB. 222 ppmC. 333 ppm 12) Calculate the Total Hardness for No. 10 A. 421.6 ppmB. 621.6 ppmC. 521.6 ppmAnalysis of an amine using a back-titration Kjeldahl method resulted in the following equation for P, the percent nitrogen in the amine: P = (mmols acid) – (mL base) (molarity base) (14.01) (100) (mg sample) = (4.75 ± 0.03 )- (0.1198) ± 0.0008) (15.00 ± 0.04) (14.01 ) (100) 750.0 ± 0.3 where the uncertainties are all standard deviations for infinite -sized samples. How will you report the value for P?A 625 mg sample of sodium bicarbonate tablet required 7.30 mL of 0.9580N sulfuric acid solution to reach the methyl red endpoint. PRELIMINARY QUESTION: Which of the following statements is/are TRUE? I. The țitrant used is sulfuric acid solution. II. The end point is a red/pink solution. III. This is an example of direct assay titration.
- 5. A 300.0 mg sample containing Na,CO3, NaHCO3 and NaOH and inert material either alone or in some combination was dissolved and titrated with 0.1000 M HCI the titration required 24.41 mL to reach the phenolphthalein endpoint. And an additional 8.67 mL to reach the methyl red endpoint. Determine the composition of the sample and calculate the percent of each titrated component.Mass of Sample Volume of KMnO, solution used in titration Equivalents of permanganate used Equivalents of iron (II) in sample Moles of iron (II) in sample Grams of Iron in Sample % Iron in Sample Average % Iron in Unknown Instructor's Grade for Precision in Part B. Sample Calculations Part B: 0.58179 0.68719 28.19 ml 31,96m6 007662 00266 2 11 nHow will the analyte concentration be altered if the titrant volume recorded is greater than required? cannot be determined from the information given It will be reported lesser than the actual concentration. It will be reported the same as the actual concentration. It will be reported greater than the actual concentration.
- True/False Indicate whether the statement is true or false. Write T if the statement is true while F if statement is false on the before each number 4.Assay of acetic acid in vinegar is an example of proximate analysis 5.Example of variable defects are color, clarity, sheen, cleanliness, smoothness, taste, and presence or absence of a characteristic. 6.Liberation of carbon dioxide during acid-alkali titration renders the analyte acidic BConcentration sodium thiosulfate solution used: 0.056 mol L-1 ACCURATE TITRATION VOLUME OF SODIUM THIOSULFATE SOLUTION USED Volume titration 1, (ml) Volume titration 2, (ml) Your Group 15.80 15.75 Group 1 16.05 15.70 Group 2 16.30 16.25 ANALYSIS Average volume used, (mL) Standard deviation Number of moles sodium thiosulfate used, (mol) Number of moles calcium iodate in solution, (mol) Volume of calcium iodate used, (mL) Concentration of saturated calcium iodate solution (mol L-¹) Unrounded value 15.9750 0.26220 Rounded value 15.97 0.262 10.0Concentration sodium thiosulfate solution used: 0.056 mol L-1 ACCURATE TITRATION VOLUME OF SODIUM THIOSULFATE SOLUTION USED Volume titration 1, (mL) Volume titration 2, (mL) Your Group 15.80 15.75 Group 1 16.05 15.70 Group 2 16.30 16.25 ANALYSIS Average volume used, (ml) Standard deviation Number of moles sodium thiosulfate used, (mol) Number of moles calcium iodate in solution, (mol) Volume of calcium iodate used, (mL) Concentration of saturated calcium iodate solution (mol L-¹) Unrounded value 15.9750 0.26220 0.00089400 0.00036700 A Rounded value 15.97 0.262 8.94 x 10-4 10.0 Minimize
- M 23 (H) Inorganic Analytical Chemistry pard My courses CHEM 23 (H) FS-AY:20-21 Week 4-5: Quantitative Analysis by Gravimetry and Titration Quiz 4 Qu 10 The 500.0-mg sample of impure Na2 CO3 (FM: 105.96) required 22.00 mL of the HCI standard solution (the obtained concentration of HCI from the previous question, problem 5: Titrimetry short answer type) for complete neutralization. ut of 1. Give the balanced chemical equation between the sample, Na2CO3 and the standard, HCI. 2. What is the mass (g) of Na, CO3 in the sample? 3. Calculate the % (w/w) purity of a 500.0-mg sample of impure Na2 CO3 Note: Type your solution here or upload its pic in Jpeg or pdf format. Another option is to send it to me via email (subject: Fam name-Quiz 4) or messenger, privately. Do not forget to box the final answer and write your name. В I 1.. 100 ml boiled cooled and filtered water sample takes 9.6 ml of M/50 EDTA in titration. The Permanent hardness of the water sample in terms of ppm of CaCO3 equivalent isCalculate the water hardness (mg L-1 of CaCO3) (i.e. calculate the mass of CaCO3) please show working out. thank you :) Sample No. 1 2 3 4 Final Burette reading (mL) 24.40 46.90 24.70 47.20 Initial Burette reading (mL) 0.10 24.40 2.10 24.70 Final-Initial Titre (mL) 24.30 22.50 22.60 22.50