Please choose an appropriate technique(s) to separate following compounds (it can be one, more than one, on none): Compound Melting Point Density Boiling Point Molar mass Phenol 40.5°C 1.07 g/cm 181.7°C 94.113 g/mol Toluene -95 °C 0.87 g/mL 111 °C 92.141 g/mol Simple Filtration Column Chromatography Distilation Crystallization/Re-Crystallization Separatory funnel None 1會云

Please choose an appropriate technique(s) to separate following compounds (it can be one, more than one, on none): Compound Melting Point Density Boiling Point Molar mass Phenol 40.5°C 1.07 g/cm 181.7°C 94.113 g/mol Toluene -95 °C 0.87 g/mL 111 °C 92.141 g/mol Simple Filtration Column Chromatography Distilation Crystallization/Re-Crystallization Separatory funnel None 1會云

Appl Of Ms Excel In Analytical Chemistry

2nd Edition

ISBN:9781285686691

Author:Crouch

Publisher:Crouch

Chapter14: Chromatography

Section: Chapter Questions

Problem 9P

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Please create a caption for this table. Solution NaCl Conc. (%) Osmolality (mOsm) % transmittance Absorbance % hemolysis % crenation C distilled 0 0 0.001029 4.987584625 100 0.03354 1 0.177179111 54.61 0.001551 4.809388202 96.42720001 0.05837 2 0.297126222 91.58 0.01012 3.994819487 80.09527231 0.08444 3 0.442542222 136.4 3.849 1.414652089 28.3634704 0.134 4 0.590164444 181.9 64.8 0.188424994 3.777880643 0.2125 5 0.74752 230.4 95.64 0.019360433 0.388172513 0.3368 6 0.89644 276.3 99.56 0.001915112 0.038397585 0.5336 7 1.095648889 337.7 99.98 8.68676E-05 0.001741676 0.9834 8 1.336711111 412 100 0 0 2.1 9 1.755568889 541.1 100 0 0 7.9 10 2.674395556 824.3 100 0 0 57.83 11 4.490211111 1384 100 0 0 99.72
Sample IdentificationCodeConcentration of M%TA=2-log(%T)Q50004.00 x 10-417.90.75Q50013.20 x 10-425.00.6Q50022.40 x 10-435.70.46Q50031.60 x 10-450.20.3Q50048.000 x 10-570.80.15SampleIdentificationCode%TA=2-log(%T)AMQ0210150143.70.359518560.360.000192Q0210150244.10.355561410.360.00018Q0210150343.80.358525890.360.00017Q0210150444.10.355561410.360.00018Q0210150543.80.358525890.360.00017What was their percent error?43%Does Batch 021015 meet legal requirements?No, because it is not between 2.85 * 10(4) and 3.15 * 10(4)Well #DropsBluedye1234567891012345678910Drops 9Distilled water876543210Concne 0.26tration0.52Test Tube #0.781.041.3Solutions3Concentration (M)2.082.32.6Concentration (ppm)1:1 dilution11.82Starting Dilution21.562:1 dilution0A.Zero standard0Was your calibration curve as linear as you expected?B.Did you experience any â€œdriftâ€ of the resistance readings?C.What is the equation of your best-fit line?D.What commercial drink did you analyze?E.Assuming…
50 Percentage Red No. 40 Soln 100% 80% 60% 40% Table 4.1: Dilutions of Red No. 40 & Absorbance Volume of Red No. 40 Soln (mL) 10me 8mL опи 4mL Percentage Red No. 40 Soln 100% 80% 60% 40% 20% Volume of DI Water (mL) OML 2mL LIML M UML 8ML Table 4.2: Dilutions of Red No. 40 & Absorbance Concentration Red No. 40 2. Report the wavelength with the maximum absorbance of Red No. 40 dye. Absorbance 20% 2ML Part A: Making a Calibration Curve for Beer's Law 1. Calculate the concentrations of each of your diluted Red No. 40 solutions and add these to Table 4.2. Show at least one sample calculation in the space below. 0.251 0.192 Total Volume 0.181 0·119 0.060 (mL) 10 mL 10 mL 10 mL 10 mL 10 mL
. Experimental data mass (g) and volume (mL) of a substance was gathering, recorded, and plotted in Figure 1. a. Correctly la bel the graph axis (include units). b. The equation for the trendline (y = mx + b) is displayed on the graph. Which variable, in the equation, equals the density of the substance? A1 feMass B D Mass Volume 2. 1,8 2,19 Mass vs. volume 3 3,15 4,08 4,13 5,57 7. 6,7 8,34 6. y= 0,794x-0.064 8 6. 10 11. 2 4. 10 13 14 15 Figure 1: Plotting of Mass vs. Volume of a Substance. bttps://www.chemisalforums.com/index.php?toric=69575.0 Life University CHM 111 March 2021 Default Page Style English (USA)
Table 1: Standardization Data Trial 1 Trial 2 O145504 Mass of KHP 04536 Initial burette reading 0.05ML 12.3 ML Final burette reading 12.8 a6.omL Volume of base used ר.12 13.2 mL Data Analysis: KH Cg Hg Da (MOIAR MASS 2041ag) 1. Calculate the molarity of base for each trial. You must use dimensional analysis – show all unit conversions (hint: start with grams of KHP used). Review the balanced equation for KHP and NaOH you wrote in Expt 11 part 1. (204.29 TRIAI 1: 0.4550g. Average: Trial 2: Trial 1: with 1875 mL of your base (use the average
A quality-control laboratory analyzes a product mixture us-ing gas-liquid chromatography. The separation of components ismore than adequate, but the process takes too long. Suggest twoways, other than changing the stationary phase, to shorten theanalysis time
ASSAY Calibration solutions Calibration solutions of naproxen in the range 5 – 25 μg/mL were prepared. Sample preparation 20 tablets weighing 12.3819 g were crushed to a fine powder. A portion of the powder (145.4 mg) was shaken with approximately 150 mL of acetic acid (0.05 M) for 5 min and then made up to volume in a 250 mL volumetric flask (stock solution). Approximately 50 mL of the stock solution was filtered and a 25 mL aliquot was diluted to 100 mL in a volumetric flask. 10 mL of the resulting solution was further diluted to 100 mL with acetic acid (0.05 M). Analysis The standards and sample solutions were analyzed by HPLC under the following conditions: Column: octadecylsilyl (ODS), 4.6 mmx150 mm, mobile phase: acetonitrile : 0.05 M acetic acid (85:15), flow rate: 1 ml/min, UV detection at 243 nm. Results: A calibration curve of concentration versus peak area was constructed for the standard solutions and gave the straight-line equation: y = 3555.6x + 85, r = 0.9999 The area…
Internal standard (As , Cs ), analyte with known concentration (Ax , Cx ) In a chromatographic equipment, a solution containing 0.006727 X and 0.008331 M S give peak area of Ax= 2316 and As= 207. To analyze an unknown sample, 5.0mL of 0.008331M S was added to 5.0mL of X, and the mixture was diluted to 50.0mL. This mixture gave a chromatography spectrum with area Ax= 3206 and As= 200. Find Cx.
o/index.html?deploymentld%3D55750828934189288909969212&elSBN=9781305657571&snapshotld%3D2199... Tp * NDTAP Q Search this co Use the References to access important values if needed for this question. Cyclopentasilane (SigH10) is a liquid with a density of 0.963 g cm3. It reacts with oxygen to give silicon dioxide (SiO2) and water. Calculate the mass of water that would form if 29.4 cm³ of cyclopentasilane reacted completely with excess oxygen. g water Submit Answer 4 question attempts remaining
Chromatography involves the separation of two or more compounds/ions caused by their molecular interactions with two phases. True False
Sample Physical Appearance 0.1 M Na2CO3 0.1 M CaCl2 Na2CO3 + CaCl2 mixture Part II filtrate + CaCl2
[References) A method for the determination of the corticosteroid methylprednisolone acetate in solutions obtained from pharmaceutical preparations yielded a mean value of 3.7 mg mL with a standard deviation of 0.3 mg mL. For quality control purposes, the relative uncertainty in the concentration should be no more than 3%. How many samples of each batch should be analyzed to ensure that the relative standard deviation does not exceed 9% at the 95% confidence level? samples