Ni content of the steel can be determined by the precipitation gravimetric analysis. For this purpose, 1.000 g of a steel sample is taken and interacted with the concentrated HCI solution. After neutralizing the resulting mixture in the presence of citrate ions, 1% dimethyl glyoxime (DMG) solution is slowly added to precipitate Ni(II) ions as Ni(DMG)2. What is the percentage of nickel in this steel sample, if 0.2269 g of Ni(DMG), (288.93 g/mol) is obtained?

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter17: Complexation And Precipitation Reactions And Titrations
Section: Chapter Questions
Problem 17.34QAP
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Ni content of the steel can be
determined by the precipitation
gravimetric analysis. For this purpose,
1.000 g of a steel sample is taken and
interacted with the concentrated HCI
solution. After neutralizing the
resulting mixture in the presence of
citrate ions, 1% dimethyl glyoxime
(DMG) solution is slowly added to
precipitate Ni(II) ions as Ni(DMG)2.
What is the percentage of nickel in this
steel sample, if 0.2269 g of Ni(DMG),
(288.93 g/mol) is obtained?
Transcribed Image Text:Ni content of the steel can be determined by the precipitation gravimetric analysis. For this purpose, 1.000 g of a steel sample is taken and interacted with the concentrated HCI solution. After neutralizing the resulting mixture in the presence of citrate ions, 1% dimethyl glyoxime (DMG) solution is slowly added to precipitate Ni(II) ions as Ni(DMG)2. What is the percentage of nickel in this steel sample, if 0.2269 g of Ni(DMG), (288.93 g/mol) is obtained?
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