nd, er Di 'H-NMR 13 C-NMR Aldehyde 10 No neighbors -singlet, IH 2 neighbor triplet, IH Imeighbor doublet, 2H C=O Gerber Acid Ester Aromatic Z neighbor triplet, 2H Aromatic C = C 126 PPM ca 2
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- How many signals would you expect each of the following molecules to have in its ¹H and ¹3C spectra? ¹H-NMR 13C-NMR Molecule #1 Babsorptions Babsorptions Molecule #2 O CH₂CCH₂CH₂CH3 absorptions absorptions Molecule #3 CH,CH,CH,CH,CHO absorptions BabsorptionsChemistry H NMR AND C13NMR ??? IN 3 CI 5 A 20= B CI 7 9Assign the two NMR spectra for the possible products Compound A: C-NMR 180 160 140 120 100 80 60 40 20 CR20120250S ppm H-NMR il 6. 4 HR20120250NS ppm
- According to this H NMR spectrum, identify the structure of the compound. the only additional information given is the molecular weight is 240.3 14 72 7.0 8 (ppm) 6.8 6.4 3.0 2.5 2.0 6 tppm)Below are the DEPT spectra for 6-methylhept-5-en-2-one. Use the information from the DEPT spectra to refine your assignments. Do the DEPT spectra help you distinguish peaks in the 13C-NMR? DEPT-135 DEPT - 90 DEPT - 45 Original Spectrum ZOO CD-3-sar 100 160 140 120 100 pom до GO 40 20 O'Η NMR 6 H 2H 2H 1 H PPM "C NMR 20 PPM Each data set is specific to an individual compound. Use the analytical data provided to come up with a structure consistent with that data.
- Consider the following 1H NMR Spectrum for the following Compound. Which proton(s) are represented by signal 1? 10 O D OC B O A OF OE 1H SIGNAL 1 -co 5H SIGNAL 2 B HH 1H 1H to D HH F HHH CE 2H SIGNAL 3 2H SIGNAL 4True or false? The NMR signal of an alcohol or amine proton often presents asa broad signal due in part to their exchangeable nature.How many H-NMR signal can be detected in this molecule?Draw the H-NMR graph please.
- Assign the peaks in the 13C NMR spectrum. Assign the peaks in the 1H NMR spectrumA sample is know to contain either hexanoic acid or 3-methylpentanoic acid. Which of the following spectra would not distinguish between the two isomers? O 'H NMR DEPT-90 O 13C NMR DEPT-135 All would distinguish between the two isomers.Consider the following 1H NMR Spectrum for the following Compound. Which proton(s) are represented by signal 4 (signal 4 is a doublet)? OA OB Of OD 09 OH 5H H 1H 1H 1H HO B D G H CH3 H HHH CEF SIGNAL HH OH 1H 2H SIGNAL SIGNAL 3 1H 1H الله 3H DONAL