Imagine you are an organic chemistry student who isolates a crude sample of salicylic acid following the Unit 2 experiment, and then you recrystallize that sample in an attempt to purify it. After a week of drying in the hood, you analyze the recrystallized product by melting point to determine purity. You divide the recrystallized product into two MP capillary tubes. You analyze Sample 1 first and then dispose of the tube and sample. After the MP apparatus has cooled, you then analyze Sample 2. You record the following data in your lab notebook: The reported literature value for pure salicylic acid is 159 °C. Sample 1 start - 157.5 °C Sample 1 end - 160.5 °C Sample 2 start - 157.3 °C Sample 2 end - 158.8 °C Using all these data, draw a conclusion about the purity of your sample (i.e., "it is pure" or "it is not pure") and explain or support your conclusion. Also provide any hypotheses you have regarding all of these data. Avoid phraseology/words such as "I feel." or "I believe." "probably" "perhaps" "possibly" or "maybe", and use "I think." or "it is hypothesized" instead. You must discuss all data in a congruent fashion.

Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
icon
Related questions
Question
Imagine you are an organic chemistry student who isolates a crude sample of salicylic acid following the Unit 2 experiment, and then you recrystallize that sample in an attempt to purify it. After a week of drying in the hood, you analyze the recrystallized product by
melting point to determine purity. You divide the recrystallized product into two MP capillary tubes. You analyze Sample 1 fırst and then dispose of the tube and sample. After the MP apparatus has cooled, you then analyze Sample 2. You record the following data in your
lab notebook:
The reported literature value for pure salicylic acid is 159 °C.
Sample 1 start = 157.5 °C
Sample 1 end = 160.5 °C
Sample 2 start = 157.3 °C
Sample 2 end = 158.8 °C
Using all these data, draw a conclusion about the purity of your sample (i.e., "it is pure" or "it is not pure") and explain or support your conclusion. Also provide any hypotheses you have regarding all of these data. Avoid phraseology/words such as "I feel..." or "I believe..",
"probably" "perhaps" "possibly" or "maybe", and use "I think.." or "it is hypothesized" instead. You must discuss all data in a congruent fashion.
Transcribed Image Text:Imagine you are an organic chemistry student who isolates a crude sample of salicylic acid following the Unit 2 experiment, and then you recrystallize that sample in an attempt to purify it. After a week of drying in the hood, you analyze the recrystallized product by melting point to determine purity. You divide the recrystallized product into two MP capillary tubes. You analyze Sample 1 fırst and then dispose of the tube and sample. After the MP apparatus has cooled, you then analyze Sample 2. You record the following data in your lab notebook: The reported literature value for pure salicylic acid is 159 °C. Sample 1 start = 157.5 °C Sample 1 end = 160.5 °C Sample 2 start = 157.3 °C Sample 2 end = 158.8 °C Using all these data, draw a conclusion about the purity of your sample (i.e., "it is pure" or "it is not pure") and explain or support your conclusion. Also provide any hypotheses you have regarding all of these data. Avoid phraseology/words such as "I feel..." or "I believe..", "probably" "perhaps" "possibly" or "maybe", and use "I think.." or "it is hypothesized" instead. You must discuss all data in a congruent fashion.
Expert Solution
steps

Step by step

Solved in 2 steps

Blurred answer
Knowledge Booster
Applications of Molecular Spectroscopy
Learn more about
Need a deep-dive on the concept behind this application? Look no further. Learn more about this topic, chemistry and related others by exploring similar questions and additional content below.
Similar questions
  • SEE MORE QUESTIONS
Recommended textbooks for you
Chemistry
Chemistry
Chemistry
ISBN:
9781305957404
Author:
Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:
Cengage Learning
Chemistry
Chemistry
Chemistry
ISBN:
9781259911156
Author:
Raymond Chang Dr., Jason Overby Professor
Publisher:
McGraw-Hill Education
Principles of Instrumental Analysis
Principles of Instrumental Analysis
Chemistry
ISBN:
9781305577213
Author:
Douglas A. Skoog, F. James Holler, Stanley R. Crouch
Publisher:
Cengage Learning
Organic Chemistry
Organic Chemistry
Chemistry
ISBN:
9780078021558
Author:
Janice Gorzynski Smith Dr.
Publisher:
McGraw-Hill Education
Chemistry: Principles and Reactions
Chemistry: Principles and Reactions
Chemistry
ISBN:
9781305079373
Author:
William L. Masterton, Cecile N. Hurley
Publisher:
Cengage Learning
Elementary Principles of Chemical Processes, Bind…
Elementary Principles of Chemical Processes, Bind…
Chemistry
ISBN:
9781118431221
Author:
Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard
Publisher:
WILEY