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I need the balanced equation and theoretical yeild of the reaction.

I need the balanced equation and theoretical yeild of the reaction.

Chemistry for Today: General, Organic, and Biochemistry
Chemistry for Today: General, Organic, and Biochemistry
9th Edition
ISBN:9781305960060
Author:Spencer L. Seager, Michael R. Slabaugh, Maren S. Hansen
Publisher:Spencer L. Seager, Michael R. Slabaugh, Maren S. Hansen
Chapter14: Aldehydes And Ketones
Section: Chapter Questions
Problem 14.38E: Glucose, the sugar present within the blood, gives a positive Benedicts test. Circle the structural...
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I need the balanced equation and theoretical yeild of the reaction.

PROCEDURE Triethylene Glycol to Ditosylate Glycol (1) 1. IN A FUMEHOOD, add 5 mL of pyridine to a large test tube. Dissolve 0.55 mL (4.03 mmol) of triethylene glycol and 0.75 g (5.22 mmol) p-toluenesulfonyl chloride in the pyridine and stir the solution for 20 minutes at room temperature. 2. Add second equivalent of 0.75 g (5.22mmol) p-toluenesulfonyl and the stir solution in warm water bath (approx. 40°C) for 1 hour and 30 minutes. 3. Remove the test tube from water bath, add 5 mL of 6 M hydrochloric acid. Place the test tube in an ice water bath and continue to stir the reaction until solid precipitates. Collect the precipitate with vacuum filtration. Allow the solid to dry on watch glass until next lab period, then collect the mass of the solid for percent yield.
Transcribed Image Text:PROCEDURE Triethylene Glycol to Ditosylate Glycol (1) 1. IN A FUMEHOOD, add 5 mL of pyridine to a large test tube. Dissolve 0.55 mL (4.03 mmol) of triethylene glycol and 0.75 g (5.22 mmol) p-toluenesulfonyl chloride in the pyridine and stir the solution for 20 minutes at room temperature. 2. Add second equivalent of 0.75 g (5.22mmol) p-toluenesulfonyl and the stir solution in warm water bath (approx. 40°C) for 1 hour and 30 minutes. 3. Remove the test tube from water bath, add 5 mL of 6 M hydrochloric acid. Place the test tube in an ice water bath and continue to stir the reaction until solid precipitates. Collect the precipitate with vacuum filtration. Allow the solid to dry on watch glass until next lab period, then collect the mass of the solid for percent yield.
explor In this experim НО. OH TSOCI pyridine TSO OTS (1) Figure 1. Synthesis of the Ditosylate Triethylene Glycol (1) from Triethylene Glycol
Transcribed Image Text:explor In this experim НО. OH TSOCI pyridine TSO OTS (1) Figure 1. Synthesis of the Ditosylate Triethylene Glycol (1) from Triethylene Glycol
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