32. Which of the following statements about tetramethylsilane is incorrect? A. it produces a single peak at 8=10 B. it is inert C. it is volatile and can be easily distilled off and used again D. it is used to provide a reference against which other peaks are measured
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- Identities of the components in a mixture may be determined by a technique called spiking. Suppose you had run a gas chromatogram on your product and had then deliberately added a drop of a known sample of 3-methylcyclohexene to a drop of your product. What would you expect the new chromatogram to show you?The melting point (mp) range of reference compound A is 320-340°C. The mp range of a 1:1 mixture of a sample of A with a sample of unknown compound B is found to be 140-300°C. Do the samples consist of identical compounds? A)Yes, because the mp of the mixture is lower than the mp of pure A. B) Not enough information is given to answer the question C) Yes, because they melt over a broad range. D) No, because the mp of the mixture is lower than the melting point of pure A.3. Correlate the structures of the standard food dyes to their relative position in the paper chromatogram. Refer to the structures shown below. *Na O H3C- OISI *Na HO CH3 Allura Red AC (pigment in red dye) N Hora O Na* O Na* O Nat O Na+ 0=8=0 HO 0=S=0 -O Na+ O Na+ Tartrazine (pigment in yellow dye) Brilliant Blue FCF (pigment in blue dye) 4. What are the identities of the unknowns in paper chromatography of food dyes? How did you arrive at this conclusion?
- 1. How does chromatography separate the components of leave samples? 2. Can you use chromatography to purify a mixture? why? 3. What is Rf value and its significance in chromatography?Use a suitable model to explain how separation and identification of a mixture of organic compounds can be achieved with a thin layer chromatographic (TLC) technique.Of the following substances, has the lowest boiling point. Select one: O CHCH2OH (M. Wt. = 46) %3D o Co2 (M. Wt = 44) O CHOCH3 (M. Wt. = 46) O CHCH NH,(M. Wt. = 45) %3D ge Next page
- Identify these statements with true or false true or false I. Chromatography utilizes partition coefficient theory true or false II. In reverse phase chromatography, the mobile phase is a polar solvent true or false I. Aspirin is an ester prodrug. true or false Aspirin is synthesized by means of an acid catalyzed reaction. true or false I. Grain alcohol boils at 78.3 C true or false Wood alcohol boils at 60 C true or false Diazo coupling involves a sigma and a pi bond in two nitrogen atoms true or false When methyl orange passes through from basic to acidic medium, the change in color is from yellow to intense red true or false Benzoic acid is a white crystalline substance that has a melting point of 122 C true or false Benzoic acid can be prepared by the alkaline reduction of toluene true or false Potassium permanganate is an oxidizing agent true or false Potassium permanganate should never be mixed with glycerin true or false Methyl…4. When performing a melting point onsolid compound using a melting point apparatus, two melting point determinations were made, One sample, which was 1 mm in height in the capillary, possessed a melting point of 133.0-133.5°C. The other sample was 10 mm in height. What would you expect the approximate melting point to be for this sample, assuming identical heating rates of 1°/min? (Hint: heat is applied from the bottom of the sample) (Give an actual numerical approximation!)(Hint: at what temperature would 1g of ice start melting at? At what temperature would 10g of ice start melting at?)How else can chromatography be used? None of these answers are correct. To wash (or remove) unwanted solvents from a mixture. To identify or exclude components in a mixture. To generate IUPAC names for hydrocarbons.
- ef Correlate the structures of the standard food dyes to their relative position in the paper chromatogram. Refer to the structures shown below. H3C. *Na O O HO. O CH3 Allura Red AC (pigment in red dye) 01510 106 FO O Nat O Nat O Nat FO O Na+ 0=8=0 HO 0=S=0 Na Na+ Tartrazine (pigment in yellow dye) Brilliant Blue FCF (pigment in blue dye) What are the identities of the unknowns in paper chromatography of food dyes? How did you arrive at this conclusion? Differentiate normal phase chromatography from reverse phase chromatography. From which of the two governs the experiment you did in thin layer chromatography of plant pigments? How do you say so?3. What is particulate gravimetry? When do we use this technique? 4. What are the conditions for a successful gravimetric analysis. 5. Define nucleation. What conditions are important for this stage.Why is the spectrophotometer set at 100% T using the FeCl3 solution rather than distilled water? O The iron chloride solution is used as the blank bećause aspirin is not soluble in distilled water. The iron chloride solution is used as the blank because distilled water will interfere with the absorbance readings. The iron chloride solution is used as the blank because that is the solvent which is present for all solutions. The iron chloride solution is used as the blank because distilled water has no color.