Standardization of 1N Potassium Hydroxide Accurately weigh about 5 g of potassium biphthalate, previously crushed lightly and dried at 120° for 2 hours, and dissolve in 75 mL of carbon dioxide-free water. Add 2 drops of phenolphthalein TS, and titrate with the sodium hydroxide solution to the production of a permanent pink color. Titration Data Weight of potassium biphthalate used in the titration: 5.1037 g Volume of potassium hydroxide solution used in the titration: 31.20 mL What is the true concentration, in normality, of the potassium hydroxide solution?
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- Sheet 5 From the following data determine the following: Define outlier and then identify the outlier in the data. Determine if the outlier should be kept of discarded from the data. Trial 1 2 3 4 HCl (mL) 22.3 28.4 29.8 29.3 NaOH (mL) 35.2 35.1 34.9 35.0Precipitimetry The chloride in a 4.321-g food sample was precipitated through the addition of 50.00 mL of a standard AgNO3 solution (10.00 mL AgNO3 = 11.22 mL KSCN). The precipitate was coated with nitrobenzene and the mixture was diluted to 250.0 mL. A 50.00 mL aliquot was taken from the diluted solution and required 4.56 mL back titration with a %3D standard KSCN solution (22.33 mL KSCN = 0.9758 g AgNO3). %3D Formula Masses: AgNO3 = 169.87; CI = 35.45 Calculate the following: 1. Molar concentration of KSCN solution M %3D 2. Molar concentration of AgNO3 solution M %3D 3. % (w/w) chloride in the original sample =Calculate the mass percent of the ascorbic acid in the same show full solution Situation: The pounded Vitamin C tablet was half into two below are the calculated data in the experiment. Each of the half are transfered in a 250ml erlen meyer flask and added 75ml of deionized water for the vitamin C to dissolve. Then it was prepared for titration where the burette was filled with 0.09794M standardize NaOH solution then a total of with 3 drops 2% phenolphthalein indicator was added to each erlen meyer flask l, swrill it and begin the titration. below are the following data gathered: Vitamins used: Nature Made vitamin C 500mg tablet Trial 1 Mass: 0.3108g of Vitamin C tablet Initial volume: 1.6mL Final volume: 15.4mL Trial 2 Mass: 0.3349g Initial volume: 15.4 mL Final volume: 30.2 mL
- Aspirin powder = 0.8110g MW of Aspirin = 180g.mol-1 Volume of 0.5N HCl consumed in back titration = 23.50mL Volume of 0.5N HCl consumed in blank titration = 44.50mL Percent purity (USP/NF) = Aspirin tablets contain NLT 90.0% and NMT 110.0% of the labeled amount of aspirin (C9H8O4) What is the calculated weight (in grams) of pure aspirin?..The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of solubility and Ksp of calcium hydroxide: Trial 2: Final Buret reading (ml)-26.10; Initial Buret reading (ml)- 19.80; Temperature (Celcius)- 25 Voume of HCl used: Trial 2- 6.30mL 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Construct an ICE table for the reaction.3. Calculate the molar solubility (in mol/L) of OH- and Ca2+.4. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 5. Calculate the Ksp of Ca(OH)26. Compute for the percent error of the experimental value for Ksp of Ca(OH)2 with the literature…SCE students measured the concentration of HCl in a solution by titrating with different indicators to find the end point.Indicator Mean HCl concentration (M)(± standard deviation)Number of measurementsBromothymol blue 0.09565 ± 0.00225 28Methyl red 0.08686 ± 0.00098 18Bromocresol green 0.08641 ± 0.00113 29Is the difference between indicators 1 and 2 significant at the 95% confidence level? Answer the same question for indicators 2 and 3
- The buret was filled with 0.100 M HCl solution. Then was transferred in a 25.0 mL of saturated calcium hydroxide solution (2g of calcium hydroxide per 100 ml of water) in two separate E-flasks. Then 2 drops of phenolphthalein was added to each flask Titration data for the determination of solubility and Ksp of calcium hydroxide: Trial 1: Final Buret reading (ml)-19.80; Initial Buret reading (ml)- 13.00; Temperature (Celcius)- 25 Trial 2: Final Buret reading (ml)-26.10; Initial Buret reading (ml)- 19.80; Temperature (Celcius)- 25 Voume of HCl used: Trial 1- 6.80ml; Trial 2- 6.30mL 1. Compute for the moles of H+ used and the moles of OH- present. moles of H+ used = (concentration of HCl) × (volume of HCl used)moles of OH- = moles of H+ used 2. Construct an ICE table for the reaction.3. Calculate the molar solubility (in mol/L) of OH- and Ca2+.4. Determine the solubility of Ca(OH)2 in g/L. (MM of Ca(OH)2 = 74.096 g/mol). 5.…The ethyl acetate concentration in an alcoholic solution was determined by diluting a 10.00-mL sample to 100.00 mL. A 20.00-mL portion of the diluted solution was refluxed with 40.00 mL of 0.04672 M KOH:CH3COOC2H5 + OH- → CH3COO- + C2H5OHAfter cooling, the excess OH2 was back-titrated with 3.41 mL of 0.05042 M H2SO4. Calculate theamount of ethyl acetate (88.11 g/mol) in the original sample in gramsA 20.330 g sample of aqueous waste leaving a fertilizer manufacturer contains ammonia. The sample is diluted with 74.044 g of water. A 10.245 g aliquot of this solution is then titrated with 0.1074 M HCl. It required 29.47 mL of the HCl solution to reach the methyl red endpoint. Calculate the weight percent NH, in the aqueous waste. wt% NH3 = APR 9 $ 4 R dº 10 % . 5 Search or type URL n T tv < 60 ♫ MacBook Pro A Y & N 7 907 U * 8 00 + I A ( 9 © | O - O W P J { + [ % ] delete
- 1. Standardization of Sodium Hydroxide Primary Standard used: Formula Mass of Primary Standard: % Purity of Primary Standard: 99.0% Trials Actual weight of Std. KHP (g) 2 3 0.8074 0.8102 0.8378 Corrected weight of KHP (g) based on % purity of primary std. Calculation of required NaOH Balanced chemical equation: Dimensional analysis:If an instrument gives a response of 1240 for a standard containing 8 ppm of a substance, how much if this substance is in a sample that gives a response of 1705? Are any assumptions needed?A 0.1475-M solution of Ba(OH)2 was used to titrate the acetic acid (60.05 g/mol) in a dilute aqueous solution. The following results were obtained. (See attached image)(a) Calculate the mean w/v percentage of acetic acid in the sample.(b) Calculate the standard deviation for the results. (Take note if n-1 should be used)(c) Calculate the 90% confidence interval for the mean.(d) (d) At the 90% confidence level, could any of the results be discarded?