A 5.12-g pesticide sample was decomposed and then dilute to 200-mL to determine its Cu²* contents. The analysis was completed by treating aliquots as indicated: Volume of sample, mL Volume of 3.82 ppm Cu²*, mL Signal 50.0 0.00 0.512 50.0 4.00 0.844 a. Calculate the percentage of copper in the pesticide sample. b. What assumption did you make in calculating the concentration of copper in your sample?
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Q: ASSAY Calibration solutions Calibration solutions of naproxen in the range 5 – 25 μg/mL were…
A: Solution- Data given- 12.3819 g were crushed to a fine powder, acetic acid (0.05 M)
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- Sample IdentificationCodeConcentration of M%TA=2-log(%T)Q50004.00 x 10-417.90.75Q50013.20 x 10-425.00.6Q50022.40 x 10-435.70.46Q50031.60 x 10-450.20.3Q50048.000 x 10-570.80.15SampleIdentificationCode%TA=2-log(%T)AMQ0210150143.70.359518560.360.000192Q0210150244.10.355561410.360.00018Q0210150343.80.358525890.360.00017Q0210150444.10.355561410.360.00018Q0210150543.80.358525890.360.00017What was their percent error?43%Does Batch 021015 meet legal requirements?No, because it is not between 2.85 * 10(4) and 3.15 * 10(4)Well #DropsBluedye1234567891012345678910Drops 9Distilled water876543210Concne 0.26tration0.52Test Tube #0.781.041.3Solutions3Concentration (M)2.082.32.6Concentration (ppm)1:1 dilution11.82Starting Dilution21.562:1 dilution0A.Zero standard0Was your calibration curve as linear as you expected?B.Did you experience any “drift†of the resistance readings?C.What is the equation of your best-fit line?D.What commercial drink did you analyze?E.Assuming…A titrimetric method for the determination of calcium in limestone was tested by analysis of an NIST limestone containing 30.15% CaO. The mean result of four analyses was 30.26% CaO, with a standard deviation of 0.085%. By pooling data from several analyses, it was established that s = 0.094% CaO.a. Do the data indicate the presence of a systematic error at the 95% confidence level?b. Do the data indicate the presence of systematic error at the 95% confidence level if no pooled value for s was available?3. At elevated temperatures, NaHCO3 is converted quantitatively to NazCO3 : 2 NaHCO3(5) = Na,CO3) + CO29) + H2O Ignition of a 0.3592 g samples containing NaHCO3 and non-volatile impurities yielded a residue weighing 0.2362g. Calculate the percent purity of the sample.
- 6. The concentration of caffeine in an energy soft drink was determined by standard addition using HPLC. The following procedure was used: a standard caffeine solution was prepared by adding 0.09850g of caffeine to 25.0 cm3 of water.A series of solutions were prepared by adding known volumes of the standard solution to the soft drink before diluting to 100 cm3. The volume of standard and the caffeine peak area are shown in the table: Energy Drink (cm3) Added caffeine Std (cm3) Peak area 15 0 965 15 5 1352 15 10 1739 15 15 2126 15 20 2513 Determine the concentration of caffeine in the soft drink as mg cm-3. A. 3.3 B. 2.3 C. 4.3 D. 7.3Following the monograph procedure, a 724-mg of aspirin (MW=180 g/mol) dissolved in 18.5 ml of cold neutralized alcohol. This solution was then initially titrated with 0.101 N sodium hydroxide solution, then later neutralized with 0.104 sulfuric acid. What is the percentage purity of the sample? 1. What is the milliequivalent weight consumed by the acidic titrant? a. 1.5392 g-meq b. 2.0907 g-meq c. 1.4948 g-meq d. 2.1528 g-meq 2. What is the milliequivalent weight consumed by the basic titrant? a. 5.8656 g-meq b. 1.5392 g-meq c. 5.6964 g-meq d. 1.4948 g-meq 3. What is the difference of milliequivalent weight consumed in the reaction? a. -4.1572 g-meq b. 4.3708 g-meq c. 0.5515 g-meq d. 4.1572 g-meqA5.12-g pesticide sample was decomposed and then dilute to 200-ml to determine its Cu2* contents. The analysis was completed by treating aliquots as indicated: Volume of sample, mL Volume of 3.82 ppm Cu2", mL Signal 50.0 0.00 0.512 50.0 4.00 0.844 a. Calculate the percentage of copper in the pesticide sample. b. What assumption did you make in calculating the concentration of copper in your sample?
- P TrueVision HD blackboard.uob.edu.bh/ultra/courses/ 19902 1/outline/assessment/ 452605 1/overview/e 1768814 1?cou Voitmeter e e salt bridge Fe KCI Cu FeSO4 CUSO,1. You wish to determine the %concentration of a stock solution of brilliant blue FCF (MW=792.8grams/mole; extinction coefficient25=97000M'cm'). You make a 1:50 dilution of stock and then you take lul from your 1:50 dilution and dilute up to 1ml in a 1cm diameter cuvette. You obtain an A625=0.1. What is your total dilution factor? What is the % concentration of the dye in the original stock?The researcher extracts a sample of well water and prepares it for TXRF analysis with a 10.00 mg/L V internal standard, like the calibration standards. The result produces SCa = 69297.81 and SV = 13481.2.Determine the concentration of Ca.
- ASSAY Calibration solutions Calibration solutions of naproxen in the range 5 – 25 μg/mL were prepared. Sample preparation 20 tablets weighing 12.3819 g were crushed to a fine powder. A portion of the powder (145.4 mg) was shaken with approximately 150 mL of acetic acid (0.05 M) for 5 min and then made up to volume in a 250 mL volumetric flask (stock solution). Approximately 50 mL of the stock solution was filtered and a 25 mL aliquot was diluted to 100 mL in a volumetric flask. 10 mL of the resulting solution was further diluted to 100 mL with acetic acid (0.05 M). Analysis The standards and sample solutions were analyzed by HPLC under the following conditions: Column: octadecylsilyl (ODS), 4.6 mmx150 mm, mobile phase: acetonitrile : 0.05 M acetic acid (85:15), flow rate: 1 ml/min, UV detection at 243 nm. Results: A calibration curve of concentration versus peak area was constructed for the standard solutions and gave the straight-line equation: y = 3555.6x + 85, r = 0.9999 The area…Table 1: Standardization Data Trial 1 Trial 2 O145504 Mass of KHP 04536 Initial burette reading 0.05ML 12.3 ML Final burette reading 12.8 a6.omL Volume of base used ר.12 13.2 mL Data Analysis: KH Cg Hg Da (MOIAR MASS 2041ag) 1. Calculate the molarity of base for each trial. You must use dimensional analysis – show all unit conversions (hint: start with grams of KHP used). Review the balanced equation for KHP and NaOH you wrote in Expt 11 part 1. (204.29 TRIAI 1: 0.4550g. Average: Trial 2: Trial 1: with 1875 mL of your base (use the averageA second spectrophotometric method for the quantitative analysis of Pb2+ in blood yields an Ssamp of 0.712 for a 5.00 mL sample of blood. After spiking the blood sample with 5.00 μL of a 1560 ppb Pb2+ external standard, an Sspike of 1.546 is measured. What is the concentration of Pb2+ in the original sample of blood?